LI Rong1a, WANG Qiang1a, ZHANG Deng-qing1a, LI Xian-ying1b, XIANG Yun-jie1a, JIN Wu-song1a
a. College of Chemistry, Chemical Engineering and Biotechnology; b. School of Environmental Science and Engineering, 1. Donghua University, Shanghai 201620, China
Abstract：2,2′-【2,5-bis｛2-［2-（2-methoxyethoxy)ethoxy］ethoxy｝-1,4-phenylene】bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane(6) was prepared by a two-step reaction from 2-［2-（2-methoxyethoxy)ethyl］-1,4-methylbenzene sulfonate. A novel phenanthroline derivative, 3,3′-【2,5-bis｛2-［2-（2-methoxyethoxy)ethoxy］ethoxy｝-1,4-phenylene】bis(1,10-phenanthrdin), was synthesized by Suzuki coupling reaction of 3-bromo-1,10-phenanthrdine with 6. The stucture was characterized by 1H NMR and MALDI-TOF-MS.
李荣， 王强， 张灯青， 李贤英， 向芸颉， 金武松. 新型邻菲啰啉衍生物的合成[J]. 合成化学, 2015, 23(12): 1147-1149.
LI Rong, WANG Qiang, ZHANG Deng-qing, LI Xian-ying, XIANG Yun-jie, JIN Wu-song. Synthesis of a Novel Phenanthroline Derivative. Chinese Journal of Synthetic Chemistry, 2015, 23(12): 1147-1149.
2015, Vol. 23 
