Abstract:A novel 2D nano-catalyst, Pd/g-C3N4NSs(1), was prepared by supporting nano-Pd on g-C3N4NSs via one-step method. The structure and morphology were characterized by TEM, XRD and XPS. The catalytic properties of 1 were investigated by Suzuki-Miyaura reaction of aryl halide with substituted phenylboronic acid. The results showed that 1 exhibited good catalytic property with 53 000 h-1 of TOF. Yield of partial products were over 99% and the catalytic performance of 1 remain stable after cycling for three times.
苏向阳, 钟琳. 新型纳米催化剂Pd/g-C3N4NSs的制备及其在Suzuki-Miyaura反应中的应用[J]. 合成化学, 2016, 24(2): 152-154.
SU Xiang-yang, ZHONG Lin. Preparation of Novel Nano-catalyst Pd/g-C3N4NSs and Its Application in Suzuki-Miyaura Reaction. Chinese Journal of Synthetic Chemistry, 2016, 24(2): 152-154.